Structures by: Palma A.

Total: 129

C64H44CoN6

C64H44CoN6

Palma, AnielloGallagher, John F.Müller-Bunz, HelgeWolowska, JoannaMcInnes, Eric J.L.O'Shea, Donal F.

Dalton Transactions (2009) 2 273-279

a=19.860(3)Å   b=44.375(5)Å   c=10.7534(13)Å

α=90.00°   β=90.00°   γ=90.00°

C64H44CuN6

C64H44CuN6

Palma, AnielloGallagher, John F.Müller-Bunz, HelgeWolowska, JoannaMcInnes, Eric J.L.O'Shea, Donal F.

Dalton Transactions (2009) 2 273-279

a=19.8465(18)Å   b=44.707(4)Å   c=10.6333(10)Å

α=90.00°   β=90.00°   γ=90.00°

C64H44N6Zn

C64H44N6Zn

Palma, AnielloGallagher, John F.Müller-Bunz, HelgeWolowska, JoannaMcInnes, Eric J.L.O'Shea, Donal F.

Dalton Transactions (2009) 2 273-279

a=19.884(2)Å   b=44.428(4)Å   c=10.7669(11)Å

α=90.00°   β=90.00°   γ=90.00°

C64H44N6Ni

C64H44N6Ni

Palma, AnielloGallagher, John F.Müller-Bunz, HelgeWolowska, JoannaMcInnes, Eric J.L.O'Shea, Donal F.

Dalton Transactions (2009) 2 273-279

a=19.842(3)Å   b=44.333(5)Å   c=10.7588(14)Å

α=90.00°   β=90.00°   γ=90.00°

(E)-3-benzoyl-2-methyl-4-(3-methylstyryl)quinoline

C26H21NO

Rodríguez, DiegoGuerrero, Sergio AndrésPalma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2020) 76, 9

a=13.2730(16)Å   b=14.8012(16)Å   c=20.137(2)Å

α=90°   β=90°   γ=90°

(E)-1-(2-Methyl-4-((E)-4-methylstyryl)quinolin-3-yl)-3- phenyl-prop-2-en-1-one

C28H23NO

Rodríguez, DiegoGuerrero, Sergio AndrésPalma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2020) 76, 9

a=10.8168(6)Å   b=17.3361(10)Å   c=12.8892(6)Å

α=90°   β=114.132(2)°   γ=90°

(<i>E</i>)-3-Acetyl-2-methyl-4-(4-methoxystyryl)quinoline

C21H19NO2

Rodríguez, DiegoGuerrero, Sergio AndrésPalma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2020) 76, 9

a=8.2595(4)Å   b=6.4279(3)Å   c=31.9064(14)Å

α=90°   β=93.674(2)°   γ=90°

(<i>E</i>)-3-Acetyl-4-(4-bromostyryl)-2-methylquinoline

C20H16BrNO

Rodríguez, DiegoGuerrero, Sergio AndrésPalma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2020) 76, 9

a=8.0849(3)Å   b=6.6692(2)Å   c=31.1063(10)Å

α=90°   β=95.0050(10)°   γ=90°

Ethyl (<i>E</i>)-4-(4-bromostyryl)-2-methylquinoline-3-carboxylate

C21H18BrNO2

Rodríguez, DiegoGuerrero, Sergio AndrésPalma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2020) 76, 9

a=9.5709(6)Å   b=10.6119(7)Å   c=18.2074(10)Å

α=90°   β=90.939(2)°   γ=90°

Ethyl (<i>E</i>)-2-methyl-4-(4-methoxystyryl)quinoline-3-carboxylate

C22H21NO3

Rodríguez, DiegoGuerrero, Sergio AndrésPalma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2020) 76, 9

a=9.5301(8)Å   b=10.3513(8)Å   c=10.3621(8)Å

α=65.374(3)°   β=86.583(3)°   γ=76.376(3)°

Ethyl (<i>E</i>)-2-methyl-4-[4-(trifluoromethyl)styryl]quinoline-3-carboxylate

C22H18F3NO2

Rodríguez, DiegoGuerrero, Sergio AndrésPalma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2020) 76, 9

a=8.7465(10)Å   b=9.9436(11)Å   c=11.1116(11)Å

α=105.446(4)°   β=99.763(4)°   γ=97.204(4)°

Ethyl 2-chloro-13-ethyl-4-oxo-8,13-dihydro-4<i>H</i>-benzo[5,6]azepino[3,2,1-<i>ij</i>]quinoline-5-carboxylate

C22H20ClNO3

Mateus-Ruíz, Jeferson B.Acosta Quintero, Lina M.Palma, AlirioMacías, Mario A.Cobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2017) 73, 1 28-35

a=6.8533(16)Å   b=10.612(5)Å   c=13.561(3)Å

α=72.45(4)°   β=75.840(19)°   γ=82.46(2)°

Ethyl 13-ethyl-4-oxo-8,13-dihydro-4<i>H</i>-benzo[5,6]azepino[3,2,1-<i>ij</i>]quinoline-5-carboxylate heptane hemisolvate

C22H21NO3,0.5(C7H16)

Macías, Mario A.Sanabria, Elkin E.Acosta-Quintero, Lina M.Palma, AlirioSuescun, Leopoldo

Acta Crystallographica Section C Structural Chemistry (2018) 74, 12

a=11.9894(3)Å   b=13.6171(4)Å   c=14.3939(4)Å

α=89.4670(13)°   β=74.3830(12)°   γ=68.1250(12)°

Methyl (2<i>RS</i>,4<i>SR</i>)-7-chloro-4-(2-chloroacetoxy)-2,3,4,5-tetrahydro-1<i>H</i>-benzo[<i>b</i>]azepine-2-carboxylate

C14H15Cl2NO4

Guerrero, Sergio A.Ramírez, Juan E.Palma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2019) 75, 2

a=8.858(6)Å   b=9.328(5)Å   c=10.526(6)Å

α=96.039(18)°   β=112.651(19)°   γ=108.99(3)°

(4a<i>RS</i>,6<i>SR</i>)-9-Chloro-6-hydroxy-4a,5,6,7-tetrahydrobenzo[<i>f</i>][1,2,4]triazino[4,5-<i>a</i>]azepin-4(3<i>H</i>)-one

C12H12ClN3O2

Guerrero, Sergio A.Ramírez, Juan E.Palma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2019) 75, 2

a=5.595(4)Å   b=8.377(5)Å   c=12.712(8)Å

α=98.10(3)°   β=100.10(2)°   γ=101.76(3)°

(4a<i>RS</i>,6<i>SR</i>)-9-chloro-6-hydroxy-3-(2-hydroxyethyl)-2,3,4a,5,6,7-hexahydrobenzo[<i>f</i>]pyrazino[1,2-<i>a</i>]azepine-1,4-dione

C15H17ClN2O4

Guerrero, Sergio A.Ramírez, Juan E.Palma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2019) 75, 2

a=9.198(6)Å   b=10.586(7)Å   c=15.223(11)Å

α=90°   β=105.56(2)°   γ=90°

(3<i>RS</i>)-4-(2-Allyl-3,5-dimethylphenyl)-1-benzyl-3-phenylpiperazine-2,5-dione

C28H28N2O2

Acosta Quintero, Lina M.Palma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2018) 74, 2

a=23.3641(8)Å   b=10.0825(3)Å   c=21.4524(7)Å

α=90°   β=115.8850(10)°   γ=90°

<i>N</i>,2,6,11-Tetramethyl-<i>N</i>-phenyl-6,11-dihydro-5<i>H</i>-benzo[<i>b</i>]pyrimido[5,4-<i>f</i>]azepin-4-amine

C22H24N4

Acosta Quintero, Lina M.Burgos, IsidroPalma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2018) 74, 3

a=11.2020(19)Å   b=16.609(3)Å   c=19.850(6)Å

α=90°   β=90°   γ=90°

5-Allyl-6-(1<i>H</i>-benzo[<i>d</i>]imidazol-1-yl)-<i>N</i>-methyl-<i>N</i>-(4-methylphenyl)pyrimidin-4-amine

C22H21N5

Acosta Quintero, Lina M.Burgos, IsidroPalma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2018) 74, 3

a=9.425(2)Å   b=11.184(3)Å   c=17.321(6)Å

α=90°   β=101.091(11)°   γ=90°

6,7,9,11-Tetramethyl-4-(5-methyl-1<i>H</i>-benzo[<i>d</i>]imidazol-1-yl)-6,11-dihydro-5<i>H</i>-benzo[<i>b</i>]pyrimido[5,4-<i>f</i>]azepine

C24H25N5

Acosta Quintero, Lina M.Burgos, IsidroPalma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2018) 74, 3

a=9.7866(13)Å   b=10.2122(15)Å   c=10.9551(14)Å

α=97.816(9)°   β=112.433(8)°   γ=94.149(8)°

Ethyl (<i>RS</i>)-13-ethyl-2-fluoro-4-oxo-8,13-dihydro-4<i>H</i>-benzo[5,6]azepino[3,2,1-<i>ij</i>]quinoline-5-carboxylate

C22H20FNO3

Acosta Quintero, Lina M.Palma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2019) 75, 6

a=9.5920(6)Å   b=13.4325(7)Å   c=14.2186(8)Å

α=90°   β=103.290(2)°   γ=90°

(<i>RS</i>)-5-Acetyl-2-chloro-11-methyl-5,6,11,12-tetrahydrobenzo[<i>b</i>,<i>f</i>]azocine

C18H18ClNO

Acosta Quintero, Lina M.Palma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2019) 75, 6

a=8.333(5)Å   b=20.800(14)Å   c=9.186(6)Å

α=90°   β=107.857(17)°   γ=90°

(6<i>RS</i>)-4-Chloro-6,11-dimethyl-6,11-dihydro-5<i>H</i>-benzo[<i>b</i>]pyrimido[5,4-<i>f</i>]azepine

C14H14ClN3

Acosta, Lina M.Jurado, JorgePalma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2015) 71, 12

a=8.6570(5)Å   b=8.8622(17)Å   c=9.0321(11)Å

α=92.649(13)°   β=113.635(9)°   γ=100.632(12)°

(6<i>RS</i>)-4-Chloro-8-methoxy-6,11-dimethyl-6,11-dihydro-5<i>H</i>-benzo[<i>b</i>]pyrimido[5,4-<i>f</i>]azepine

C15H16ClN3O

Acosta, Lina M.Jurado, JorgePalma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2015) 71, 12

a=8.2148(7)Å   b=12.9078(8)Å   c=15.0778(6)Å

α=90°   β=122.774(5)°   γ=90°

(6<i>RS</i>)-4-Chloro-8-hydroxy-6,11-dimethyl-6,11-dihydro-5<i>H</i>-benzo[<i>b</i>]pyrimido[5,4-<i>f</i>]azepine

C14H14ClN3O

Acosta, Lina M.Jurado, JorgePalma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2015) 71, 12

a=8.0251(7)Å   b=21.5510(17)Å   c=8.0709(6)Å

α=90°   β=116.216(6)°   γ=90°

(6<i>RS</i>)-4-Chloro-8-methoxy-6,11-dimethyl-2-phenyl-6,11-dihydro-5<i>H</i>-benzo[<i>b</i>]pyrimido[5,4-<i>f</i>]azepine

C21H20ClN3O

Acosta, Lina M.Jurado, JorgePalma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2015) 71, 12

a=13.9431(8)Å   b=9.2078(10)Å   c=14.802(4)Å

α=90°   β=106.521(8)°   γ=90°

(RS)-8-chloro-6-methyl-1,2,6,7-tetrahydropyrimido[5',4':6,7]azepino[3,2,1-hi]indole

C15H14ClN3

Acosta Quintero, Lina M.Burgos, IsidroPalma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2016) 72, 1 52-56

a=6.6250(3)Å   b=22.4796(13)Å   c=8.6355(4)Å

α=90°   β=100.610(3)°   γ=90°

(RS)-9-chloro-7-methyl-2,3,7,8-tetrahydro-1H-pyrimido[5',4':6,7]azepino[3,2,1-ij]-quinoline

C16H16ClN3

Acosta Quintero, Lina M.Burgos, IsidroPalma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2016) 72, 1 52-56

a=8.1840(10)Å   b=9.5399(12)Å   c=10.2185(19)Å

α=104.471(7)°   β=101.049(6)°   γ=111.324(5)°

(6<i>RS</i>,11<i>RS</i>)-11-Ethyl-6,11-dihydro-5<i>H</i>-dibenzo[<i>b</i>,<i>e</i>]azepine-6-carboxamide

C17H18N2O

Acosta Quintero, Lina M.Palma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2016) 72, 7 549-554

a=5.6051(2)Å   b=8.6411(3)Å   c=14.3853(6)Å

α=86.192(2)°   β=81.237(3)°   γ=87.313(2)°

(2<i>RS</i>)-2,8-Dimethyl-4-phenyl-1,2-dihydro-6<i>H</i>-pyrrolo[3,2,1-<i>ij</i>]quinolin-6-one

C19H17NO

Luque, Adriana L.Sanabria, Carlos M.Palma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2016) 72, 8

a=17.756(5)Å   b=10.364(3)Å   c=15.232(4)Å

α=90°   β=92.774(8)°   γ=90°

(2<i>SR</i>,4<i>RS</i>)-6,8-Dimethyl-2-(naphthalen-1-yl)-2,3,4,5-tetrahydro-1<i>H</i>-1,4-epoxy-1-benzazepine

C22H21N1O1

Macías, Mario A.Acosta, Lina M.Sanabria, Carlos M.Palma, AlirioRoussel, PascalGauthier, Gilles H.Suescun, Leopoldo

Acta Crystallographica Section C (2016) 72, 5 363-372

a=24.8049(10)Å   b=10.7126(5)Å   c=12.1932(4)Å

α=90°   β=95.9290(10)°   γ=90°

7-Fluoro-<i>cis</i>-2-[(<i>E</i>)-styryl]-2,3,4,5-tetrahydro-1<i>H</i>-1-\ benzazepin-4-ol

C18H18FNO

Macías, Mario A.Acosta, Lina M.Sanabria, Carlos M.Palma, AlirioRoussel, PascalGauthier, Gilles H.Suescun, Leopoldo

Acta Crystallographica Section C (2016) 72, 5 363-372

a=7.5932(3)Å   b=7.5859(4)Å   c=51.010(3)Å

α=90°   β=90°   γ=90°

7-Fluoro-<i>cis</i>-2-[(<i>E</i>)-pent-1-enyl]-2,3,4,5-tetrahydro-1<i>H</i>-1-benzazepin-4-ol

C15H20FNO

Macías, Mario A.Acosta, Lina M.Sanabria, Carlos M.Palma, AlirioRoussel, PascalGauthier, Gilles H.Suescun, Leopoldo

Acta Crystallographica Section C (2016) 72, 5 363-372

a=25.119(2)Å   b=25.119(2)Å   c=11.2812(12)Å

α=90°   β=90°   γ=120°

7-Fluoro-<i>cis</i>-2-[(<i>E</i>)-pent-1-enyl]-2,3,4,5-tetrahydro-1<i>H</i>-1-benzazepin-4-ol

C15H20FNO

Macías, Mario A.Acosta, Lina M.Sanabria, Carlos M.Palma, AlirioRoussel, PascalGauthier, Gilles H.Suescun, Leopoldo

Acta Crystallographica Section C (2016) 72, 5 363-372

a=49.395(2)Å   b=49.395(2)Å   c=11.1802(5)Å

α=90°   β=90°   γ=120°

6,11-Dimethyl-3,5,6,11-tetrahydro-4<i>H</i>-benzo[<i>b</i>]pyrimido[5,4-<i>f</i>]azepin-4-one

C14H15N3O

Acosta Quintero, Lina M.Palma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2016) 72, 4 346-357

a=17.0839(16)Å   b=4.2350(3)Å   c=16.2258(18)Å

α=90°   β=94.047(8)°   γ=90°

4-Butoxy-6,11-dimethyl-6,11-dihydro-5<i>H</i>-benzo[<i>b</i>]pyrimido[5,4-<i>f</i>]azepin-8-ol

C18H23N3O2

Acosta Quintero, Lina M.Palma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2016) 72, 4 346-357

a=11.4233(4)Å   b=7.3707(3)Å   c=20.4624(7)Å

α=90°   β=93.561(2)°   γ=90°

<i>N</i>-Benzyl-6-methyl-1,2,6,7-tetrahydropyrimido\ [5,4':6,7]azepino[3,2,1-<i>hi</i>]indol-8-amine

C22H22N4

Acosta Quintero, Lina M.Palma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2016) 72, 4 346-357

a=7.7594(4)Å   b=8.5383(6)Å   c=13.4525(8)Å

α=90°   β=100.483(3)°   γ=90°

<i>N</i>-Benzyl-8-methoxy-6,11-dimethyl-6,11-dihydro-5<i>H</i>- benzo[<i>b</i>]pyrimido[5,4-<i>f</i>]azepin-4-amine

C22H24N4O

Acosta Quintero, Lina M.Palma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2016) 72, 4 346-357

a=12.2994(8)Å   b=9.1501(5)Å   c=16.1710(9)Å

α=90°   β=95.289(2)°   γ=90°

4-Dimethylamino-6,11-dimethyl-6,11-dihydro-5<i>H</i>-\ benzo[<i>b</i>]pyrimido[5,4-<i>f</i>]azepin-8-ol

C16H20N4O

Acosta Quintero, Lina M.Palma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2016) 72, 4 346-357

a=18.886(3)Å   b=7.9898(15)Å   c=19.335(3)Å

α=90°   β=90°   γ=90°

<i>N</i>-Benzyl-7-methyl-2,3,7,8-tetrahydro-1<i>H</i>-\ pyrimido[5,4':6,7]azepino[3,2,1-<i>ij</i>]quinolin-9-amine

C23H24N4

Acosta Quintero, Lina M.Palma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2016) 72, 4 346-357

a=15.083(3)Å   b=27.563(4)Å   c=8.8681(13)Å

α=90°   β=90°   γ=90°

4,4'-(Phenylmethylene)bis(6-allyl-3-chloro-2-methylaniline)

C27H28Cl2N2

Blanco, Maria C.Palma, AlirioBahsas, AliHursthouse, Michael B.Cobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2009) 65, 9 o479-o482

a=8.9868(2)Å   b=10.8718(4)Å   c=12.4359(4)Å

α=94.333(2)°   β=93.634(3)°   γ=102.490(2)°

(2<i>RS</i>,4<i>SR</i>)-2-<i>exo</i>-(5-bromo-2-thienyl)-7-chloro- 2,3,4,5-tetrahydro-1<i>H</i>-1,4-epoxy-1-benzazepine

C14H11BrClNOS

Blanco, Maria C.Palma, AlirioBahsas, AliCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2009) 65, 9 o487-o491

a=10.7959(11)Å   b=14.2116(16)Å   c=17.4303(11)Å

α=90.00°   β=90.00°   γ=90.00°

4,4'-(2-thienylmethylene)bis(6-allyl-3-chloro-2-methylaniline)

C25H26Cl2N2S

Blanco, Maria C.Palma, AlirioBahsas, AliHursthouse, Michael B.Cobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2009) 65, 9 o479-o482

a=8.7263(2)Å   b=10.6766(2)Å   c=12.2691(3)Å

α=77.1100(10)°   β=87.7930(10)°   γ=82.367(2)°

(2<i>RS</i>,4<i>SR</i>)-2-<i>exo</i>-(5-methyl-2-thienyl)-2,3,4,5- tetrahydro-1<i>H</i>-1,4-epoxy-1-benzazepine

C15H15NOS

Blanco, Maria C.Palma, AlirioBahsas, AliCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2009) 65, 9 o487-o491

a=8.3789(12)Å   b=9.6964(14)Å   c=30.952(4)Å

α=90.00°   β=90.00°   γ=90.00°

(2<i>RS</i>,4<i>SR</i>)-7-chloro-2-<i>exo</i>-(5-methyl-2-thienyl)- 2,3,4,5-tetrahydro-1<i>H</i>-1,4-epoxy-1-benzazepine

C15H14ClNOS

Blanco, Maria C.Palma, AlirioBahsas, AliCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2009) 65, 9 o487-o491

a=15.042(3)Å   b=15.739(3)Å   c=5.6216(13)Å

α=90.00°   β=100.120(16)°   γ=90.00°

(2<i>RS</i>,4<i>SR</i>)-7-Bromo-2-(2-methylphenyl)-2,3,4,5-tetrahydro-1<i>H</i>-naphtho[1,2-<i>b</i>]azepin-4-ol

C21H20BrNO

Yépes, Andrés F.Palma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2013) 69, 4 448-452

a=8.438(2)Å   b=24.957(5)Å   c=16.221(4)Å

α=90.00°   β=93.914(16)°   γ=90.00°

(2<i>RS</i>,4<i>SR</i>)-2-(3-Methylthiophen-2-yl)-2,3,4,5-tetrahydro-1<i>H</i>-naphtho[1,2-<i>b</i>]azepin-4-ol

C19H19NOS

Yépes, Andrés F.Palma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2013) 69, 4 448-452

a=25.431(5)Å   b=16.318(3)Å   c=8.0193(6)Å

α=90.00°   β=104.021(10)°   γ=90.00°

(2<i>R</i>*,4<i>S</i>*)-2-(Pyridin-3-yl)-2,3,4,5-tetrahydro-1<i>H</i>- 1-benzazepin-4-ol

C15H16N2O

Gómez, Sandra L.Palma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2011) 67, 5 o157-o160

a=6.0318(9)Å   b=8.3396(10)Å   c=25.361(4)Å

α=90.00°   β=90.00°   γ=90.00°

(2<i>R</i>*,4<i>S</i>*)-Methyl 4-hydroxy-2,3,4,5-tetrahydro-1<i>H</i>-benz[<i>b</i>]azepine-2-carboxylate

C12H15NO3

Guerrero, Sergio A.Sanabría, Carlos M.Palma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2014) 70, 4 408-415

a=6.2528(13)Å   b=10.758(3)Å   c=15.927(5)Å

α=90.00°   β=90.00°   γ=90.00°

(2<i>R</i>*,4<i>S</i>*)-Methyl 2,3,4,5-tetrahydro-1,4-epoxy-1<i>H</i>-benz[<i>b</i>]azepine-2-carboxylate

C12H13NO3

Guerrero, Sergio A.Sanabría, Carlos M.Palma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2014) 70, 4 408-415

a=6.8549(6)Å   b=11.4483(12)Å   c=13.1369(14)Å

α=90.00°   β=90.00°   γ=90.00°

(2<i>RS</i>,4<i>SR</i>)-4-Hydroxy-2,3,4,5-tetrahydro-1<i>H</i>-benz[<i>b</i>]azepine-2-carboxylic acid

C11H13NO3

Guerrero, Sergio A.Sanabría, Carlos M.Palma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2014) 70, 4 408-415

a=9.4389(5)Å   b=11.9081(5)Å   c=9.2702(4)Å

α=90.00°   β=108.275(3)°   γ=90.00°

(6<i>R</i>*,11<i>R</i>*)-5-Acetyl-11-ethyl-6,11-dihydro-5<i>H</i>-dibenzo[<i>b</i>,<i>e</i>]azepine-6-carboxylic acid

C19H19NO3

Sanabría, Carlos M.Palma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2014) 70, 3 332-337

a=8.8053(3)Å   b=10.9821(4)Å   c=9.0080(6)Å

α=90.00°   β=118.510(3)°   γ=90.00°

(6<i>RS</i>,11<i>SR</i>)-5-Acetyl-11-ethyl-2-methyl-6,11-dihydro-\ 5<i>H</i>-dibenzo[<i>b</i>,<i>e</i>]azepine-6-carboxylic acid

C20H21NO3

Sanabría, Carlos M.Palma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2014) 70, 3 332-337

a=15.2894(16)Å   b=10.760(2)Å   c=10.538(2)Å

α=90.00°   β=100.990(11)°   γ=90.00°

(6<i>RS</i>,11<i>SR</i>)-5-Acetyl-11-ethyl-1,3-dimethyl-6,11-dihydro-\ 5<i>H</i>-dibenzo[<i>b</i>,<i>e</i>]azepine-6-carboxylic acid

C21H23NO3

Sanabría, Carlos M.Palma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2014) 70, 3 332-337

a=9.2283(11)Å   b=16.691(2)Å   c=11.9824(18)Å

α=90.00°   β=103.820(11)°   γ=90.00°

7,9-dichloro-2-<i>exo</i>-(prop-1-en-2-yl)-2,3,4,5-tetrahydro- 1<i>H</i>-1,4-epoxy-1-benzazepine

C13H13Cl2NO

Acosta, Lina M.Palma, AlirioBahsas, AliCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2010) 66, 4 o209-o214

a=10.4753(13)Å   b=5.4759(8)Å   c=10.9632(12)Å

α=90.00°   β=105.791(13)°   γ=90.00°

(2<i>SR</i>,4<i>RS</i>)-2-<i>exo</i>-vinyl-2,3,4,5-tetrahydro-1<i>H</i>- 1,4-epoxy-1-benzazepine

C12H13NO

Acosta, Lina M.Palma, AlirioBahsas, AliCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2010) 66, 4 o209-o214

a=9.8070(13)Å   b=7.3982(7)Å   c=13.738(2)Å

α=90.00°   β=105.441(11)°   γ=90.00°

(2<i>SR</i>,4<i>RS</i>)-8-chloro-9-methyl-2-<i>exo</i>-(2-methylprop-1-enyl)- 2,3,4,5-tetrahydro-1<i>H</i>-1,4-epoxy-1-benzazepine

C15H18ClNO

Acosta, Lina M.Palma, AlirioBahsas, AliCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2010) 66, 4 o209-o214

a=11.0631(7)Å   b=5.7212(5)Å   c=21.203(6)Å

α=90.00°   β=102.587(16)°   γ=90.00°

(2<i>SR</i>,4<i>RS</i>)-8-chloro-9-methyl-2-<i>exo</i>-(prop-1-en-2-yl)- 2,3,4,5-tetrahydro-1<i>H</i>-1,4-epoxy-1-benzazepine

C14H16ClNO

Acosta, Lina M.Palma, AlirioBahsas, AliCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2010) 66, 4 o209-o214

a=8.6828(11)Å   b=10.1456(6)Å   c=14.2976(16)Å

α=90.000°   β=107.587(9)°   γ=90.000°

2-exo-phenyl-2,3,4,5-tetrahydro-1<i>H</i>-1,4-epoxy-1-benzazepine

C16H15NO

Gómez, Sandra L.Palma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2010) 66, 4 o233-o240

a=10.7475(7)Å   b=10.7842(12)Å   c=20.5812(19)Å

α=90.00°   β=91.688(7)°   γ=90.00°

(<i>2RS</i>,4<i>SR</i>)-2-(5-bromothiophen-2-yl)-2,3,4,5-tetrahydro-1,4-epoxynaphtho[1,2-<i>b</i>]azepine

C18H14BrNOS

Yépes, Andrés F.Palma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2013) 69, 3 307-312

a=15.316(2)Å   b=9.9230(18)Å   c=20.225(3)Å

α=90.000°   β=90.000°   γ=90.000°

Ethyl 3-amino-<i>N</i>-{2-amino-5-formyl-6-[methyl(phenyl)amino]pyrimidin- 4-yl}propionate

C17H21N5O3

Acosta, Lina M.Yepes, Andrés F.Palma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2013) 69, 2 162-171

a=16.707(6)Å   b=10.218(2)Å   c=20.733(5)Å

α=90.00°   β=105.929(19)°   γ=90.00°

<i>N</i>-{2-Amino-5-formyl-6-[methyl(phenyl)amino]pyrimidin-4-yl}glycinamide

C14H16N6O2

Acosta, Lina M.Yepes, Andrés F.Palma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2013) 69, 2 162-171

a=20.045(4)Å   b=8.6868(7)Å   c=17.990(3)Å

α=90.00°   β=114.064(11)°   γ=90.00°

Ethyl <i>N</i>-{2-amino-5-formyl-6-[methyl(phenyl)amino]pyrimidin-4-yl}glycinate

C16H19N5O3

Acosta, Lina M.Yepes, Andrés F.Palma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2013) 69, 2 162-171

a=7.3990(5)Å   b=9.609(3)Å   c=12.449(3)Å

α=73.30(2)°   β=82.680(14)°   γ=72.693(13)°

Methyl <i>N</i>-{2-amino-6-[benzyl(methyl)amino]-5-formylpyrimidin-4-yl}glycinate

C16H19N5O3

Acosta, Lina M.Yepes, Andrés F.Palma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2013) 69, 2 162-171

a=15.636(4)Å   b=6.5674(18)Å   c=17.336(5)Å

α=90.00°   β=113.440(18)°   γ=90.00°

Ethyl 3-amino-<i>N</i>-[2-amino-5-formyl-6-(piperidin-4-yl)pyrimidin-4-yl]propionate

C15H23N5O3

Acosta, Lina M.Yepes, Andrés F.Palma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2013) 69, 2 162-171

a=8.040(4)Å   b=10.391(3)Å   c=10.458(8)Å

α=109.16(3)°   β=98.19(5)°   γ=103.10(3)°

(2<i>R</i>,4<i>S</i>)-2-(3-Methylthiophen-2-yl)-2,3,4,5-tetrahydro-1,4-epoxynaphtho[1,2-<i>b</i>]-azepine

C19H17NOS

Yépes, Andrés F.Palma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2013) 69, 3 307-312

a=7.0387(3)Å   b=11.5605(10)Å   c=18.1951(17)Å

α=90.00°   β=90.00°   γ=90.00°

(2<i>RS</i>,4<i>SR</i>)-2-(5-Methylthiophen-2-yl)-2,3,4,5-tetrahydro-1,4-epoxy-naphtho[1,2-<i>b</i>]azepine

C19H17NOS

Yépes, Andrés F.Palma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2013) 69, 3 307-312

a=16.165(2)Å   b=5.2505(3)Å   c=20.0410(19)Å

α=90.00°   β=118.813(9)°   γ=90.00°

(2<i>R</i>,4<i>S</i>)-7-Bromo-2-phenyl-2,3,4,5-tetrahydro-1,4- epoxynaphtho[1,2-<i>b</i>]azepine

C20H16BrNO

Palma, AlirioBahsas, AliYépes, Andrés F.Cobo, JustoHursthouse, Michael B.Glidewell, Christopher

Acta Crystallographica Section C (2009) 65, 4 o140-o145

a=7.8444(3)Å   b=9.8146(4)Å   c=10.0871(4)Å

α=90.00°   β=92.103(3)°   γ=90.00°

4-Hydroxy-2-vinyl-2,3,4,5-tetrahydro-1-benzazepine

C12H15NO

Acosta, Lina M.Bahsas, AliPalma, AlirioCobo, JustoHursthouse, Michael B.Glidewell, Christopher

Acta Crystallographica Section C (2009) 65, 3 o92-o96

a=10.3466(13)Å   b=7.488(3)Å   c=13.227(9)Å

α=90.00°   β=92.94(2)°   γ=90.00°

7-fluoro-4-hydroxy-2-vinyl-2,3,4,5-tetrahydro-1-benzazepine

C12H14FNO

Acosta, Lina M.Bahsas, AliPalma, AlirioCobo, JustoHursthouse, Michael B.Glidewell, Christopher

Acta Crystallographica Section C (2009) 65, 3 o92-o96

a=10.5258(13)Å   b=7.4501(13)Å   c=13.251(2)Å

α=90.00°   β=93.441(2)°   γ=90.00°

(2RS,4SR)-7-bromo-2-(4-chlorophenyl-2,3,4,5-tetrahydro- 1,4-epoxynaphtho[1,2-<i>b</i>]azepine

C20H15BrClNO

Palma, AlirioBahsas, AliYépes, Andrés F.Cobo, JustoHursthouse, Michael B.Glidewell, Christopher

Acta Crystallographica Section C (2009) 65, 4 o140-o145

a=9.7758(16)Å   b=9.8211(14)Å   c=33.174(3)Å

α=90.000°   β=90.000°   γ=90.000°

(2RS,4SR)-2-(4-fluorophenyl)-2,3,4,5-tetrahydro-1,4- epoxynaphtho[1,2-<i>b</i>]azepine

C20H16FNO

Palma, AlirioBahsas, AliYépes, Andrés F.Cobo, JustoHursthouse, Michael B.Glidewell, Christopher

Acta Crystallographica Section C (2009) 65, 4 o140-o145

a=11.3036(4)Å   b=12.7585(5)Å   c=11.1730(3)Å

α=90.00°   β=109.137(2)°   γ=90.00°

(2<i>S</i>,4<i>R</i>)-2-<i>exo</i>-(2-Chlorophenyl)-2,3,4,5-tetrahydro- 1<i>H</i>-1,4-epoxy-1-benzazepine

C16H14ClNO

Gómez, Sandra L.Sanabria, Carlos M.Palma, AlirioBahsas, AliCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2009) 65, 9 o465-o469

a=8.8558(19)Å   b=7.3585(13)Å   c=9.9622(18)Å

α=90.00°   β=101.622(17)°   γ=90.00°

(2<i>SR</i>,4<i>RS</i>)-2-<i>exo</i>-(2-Chloro-6-fluorophenyl)-2,3,4,5- tetrahydro-1<i>H</i>-1,4-epoxy-1-benzazepine

C16H13ClFNO

Gómez, Sandra L.Sanabria, Carlos M.Palma, AlirioBahsas, AliCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2009) 65, 9 o465-o469

a=9.0768(13)Å   b=10.9461(9)Å   c=12.9971(18)Å

α=90.00°   β=99.768(9)°   γ=90.00°

(2<i>SR</i>,4<i>RS</i>)-7-methyl-2-<i>exo</i>-(4-methylphenyl)- 2,3,4,5-tetrahydro-1<i>H</i>-1,4-epoxy-1-benzazepine

C18H19NO

Gómez, Sandra L.Sanabria, Carlos M.Palma, AlirioBahsas, AliCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2009) 65, 9 o465-o469

a=9.7687(9)Å   b=10.3022(17)Å   c=14.239(2)Å

α=90.00°   β=108.222(10)°   γ=90.00°

C17H16ClNO

C17H16ClNO

Gómez, Sandra L.Sanabria, Carlos M.Palma, AlirioBahsas, AliCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2009) 65, 9 o465-o469

a=8.7150(9)Å   b=10.406(2)Å   c=15.312(4)Å

α=99.547(19)°   β=90.621(14)°   γ=96.514(13)°

7-bromo-2-exo-phenyl-2,3,4,5-tetrahydro-1<i>H</i>-1,4- epoxy-1-benzazepine

C16H14BrNO

Gómez, Sandra L.Palma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2010) 66, 4 o233-o240

a=5.5214(3)Å   b=10.2982(12)Å   c=22.900(3)Å

α=90.00°   β=90.00°   γ=90.00°

(2<i>S</i>,4<i>R</i>)-7-fluoro-2-<i>exo</i>-[(<i>E</i>)-styryl]-2,3,4,5-\ tetrahydro-1<i>H</i>-1,4-epoxy-1-benzazepine

C18H16FNO

Acosta, Lina M.Palma, AlirioBahsas, AliCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2010) 66, 4 o206-o208

a=10.052(4)Å   b=5.299(4)Å   c=12.976(8)Å

α=90.00°   β=91.10(4)°   γ=90.00°

2-exo-(4-chlorophenyl)-2,3,4,5-tetrahydro-1<i>H</i>- 1,4-epoxy-1-benzazepine

C16H14ClNO

Gómez, Sandra L.Palma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2010) 66, 4 o233-o240

a=8.2405(14)Å   b=11.5432(16)Å   c=27.442(2)Å

α=90.00°   β=101.030(13)°   γ=90.00°

2-exo-(3-methylphenyl)-2,3,4,5-tetrahydro-1<i>H</i>-1,4- epoxy-1-benzazepine

C17H17NO

Gómez, Sandra L.Palma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2010) 66, 4 o233-o240

a=10.9966(17)Å   b=23.691(10)Å   c=10.6323(8)Å

α=90.00°   β=111.661(8)°   γ=90.00°

2-exo-(4-bromophenyl)-7-chloro-2,3,4,5- tetrahydro-1<i>H</i>-1,4-epoxy-1-benzazepine

C16H13BrClNO

Gómez, Sandra L.Palma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2010) 66, 4 o233-o240

a=15.3626(16)Å   b=11.5436(13)Å   c=7.8832(13)Å

α=90.00°   β=96.080(11)°   γ=90.00°

(2<i>RS</i>,4<i>RS</i>)-8-chloro-9-methyl-2-<i>endo</i>-(2-methylprop-1-enyl)- 2,3,4,5-tetrahydro-1<i>H</i>-1,4-epoxy-1-benzazepine

C15H18ClNO

Acosta, Lina M.Palma, AlirioBahsas, AliCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2010) 66, 4 o209-o214

a=5.2890(9)Å   b=9.3076(16)Å   c=13.551(3)Å

α=94.554(15)°   β=94.684(15)°   γ=97.298(14)°

(2<i>SR</i>,4<i>RS</i>)-7-chloro-2-<i>exo</i>-(2-methylprop-1-enyl)- 2,3,4,5-tetrahydro-1<i>H</i>-1,4-epoxy-1-benzazepine

C14H16ClNO

Acosta, Lina M.Palma, AlirioBahsas, AliCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2010) 66, 4 o209-o214

a=5.6445(5)Å   b=25.744(3)Å   c=8.3894(11)Å

α=90.00°   β=95.124(9)°   γ=90.00°

5-Acetyl-2-chloro-8,11-dimethyl-5,6,11,12- tetrahydrodibenzo[<i>b</i>,<i>f</i>]azocine

C19H20ClNO

Yepes, Andrés F.Jaimes, EdersonBahsas, AliPalma, AlirioHursthouse, Michael B.Cobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2010) 66, 6 o284-o288

a=8.3396(3)Å   b=21.7131(7)Å   c=9.2010(3)Å

α=90.00°   β=106.683(2)°   γ=90.00°

(2SR,4RS)-7-Chloro-2-<i>exo</i>-[(<i>E</i>)-styryl]-2,3,4,5-tetrahydro- 1,4-epoxy-1H-1-benzazepine

C18H16ClNO

Acosta, Lina M.Bahsas, AliPalma, AlirioCobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section C (2008) 64, 9 o514-o518

a=10.5798(8)Å   b=5.3448(10)Å   c=12.873(3)Å

α=90.00°   β=90.204(12)°   γ=90.00°

(2RS,4RS)-7-Chloro-2-<i>endo</i>-[(<i>E</i>)-styryl]-2,3,4,5-tetrahydro- 1,4-epoxy-1H-1-benzazepine

C18H16ClNO

Acosta, Lina M.Bahsas, AliPalma, AlirioCobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section C (2008) 64, 9 o514-o518

a=5.2855(10)Å   b=15.649(2)Å   c=17.880(3)Å

α=90.00°   β=90.00°   γ=90.00°

(2<i>R</i>,4<i>R</i>)-7-fluoro-2-endo-[(<i>E</i>)-styryl]-2,3,4,5-tetrahydro- 1,4-epoxy-1H-1-benzazepine

C18H16FNO

Acosta, Lina M.Bahsas, AliPalma, AlirioCobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section C (2008) 64, 9 o514-o518

a=5.4172(2)Å   b=8.0164(6)Å   c=16.2310(11)Å

α=90.00°   β=96.745(4)°   γ=90.00°

(2<i>S</i>,4<i>R</i>)-2-<i>exo</i>-(5-bromo-2-thienyl)-7-trifluoromethoxy- 2,3,4,5-tetrahydro-1H-1,4-epoxy-1-benzazepine

C15H11BrF3NO2S

Blanco, Maria C.Raysth, WalterPalma, AlirioCobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section C (2008) 64, 9 o524-o528

a=5.6913(6)Å   b=10.1187(6)Å   c=13.2996(13)Å

α=90.00°   β=100.497(8)°   γ=90.00°

(2<i>S</i>,4<i>R</i>)-7-chloro-2-<i>exo</i>-(2-chlorophenyl)- 2,3,4,5-tetrahydro-1H-1,4-epoxy-1-benzazepine

C16H13Cl2NO

Gómez, Sandra L.Raysth, WalterPalma, AlirioCobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section C (2008) 64, 9 o519-o523

a=7.4328(11)Å   b=12.3746(16)Å   c=14.9187(19)Å

α=90.00°   β=90.00°   γ=90.00°

(2<i>S</i>,4<i>R</i>)-7-chloro-2-<i>exo</i>- (1-naphthyl)-2,3,4,5-tetrahydro-1H-1,4-epoxy-1-benzazepine

C20H16ClNO

Gómez, Sandra L.Raysth, WalterPalma, AlirioCobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section C (2008) 64, 9 o519-o523

a=9.6174(18)Å   b=11.558(3)Å   c=13.465(4)Å

α=90.00°   β=90.00°   γ=90.00°

(2SR,4RS)-2-<i>exo</i>-(5-bromo-2-thienyl)-7-fluoro- 2,3,4,5-tetrahydro-1H-1,4-epoxy-1-benzazepine

C14H11BrFNOS

Blanco, Maria C.Raysth, WalterPalma, AlirioCobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section C (2008) 64, 9 o524-o528

a=8.1835(6)Å   b=10.9447(8)Å   c=14.6940(12)Å

α=90.00°   β=104.969(6)°   γ=90.00°

(2SR,4RS)-7-Fluoro-2-<i>exo</i>-(2-furyl)-2,3,4,5-tetrahydro-1H-1,4-epoxy- 1-benzazepine

C14H12FNO2

Blanco, Maria C.Raysth, WalterPalma, AlirioCobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section C (2008) 64, 9 o524-o528

a=5.5314(10)Å   b=15.430(4)Å   c=26.229(6)Å

α=90.00°   β=92.960(17)°   γ=90.00°

(2SR,4RS)-7-chloro-2-<i>exo</i>-(4-chlorophenyl)-2,3,4,5-tetrahydro- 1H-1,4-epoxy-1-benzazepine

C16H13Cl2NO

Gómez, Sandra L.Raysth, WalterPalma, AlirioCobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section C (2008) 64, 9 o519-o523

a=11.9348(11)Å   b=21.617(2)Å   c=5.3024(6)Å

α=90.00°   β=90.00°   γ=90.00°

(2<i>S</i>*,4<i>R</i>*)-2-<i>exo</i>-(1-Naphthyl)-7-trifluoromethyl-2,3,4,5- tetrahydro-1<i>H</i>-1,4-epoxy-1-benzazepine

C21H16F3NO2

Sanabria, Carlos M.Gómez, Sandra L.Palma, AlirioCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2010) 66, 11 o540-o546

a=7.2209(5)Å   b=13.140(2)Å   c=17.559(2)Å

α=90.00°   β=90.00°   γ=90.00°